adipdic acid – Flashcards

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Adipdic acid
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To synthesize idiotic acid from cyclohexene through oxidative cleavage (results confirmed by IR)
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Vertaldehyde oxime
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To synthesize veratraldehyde from veretraldehyde (results confirmed by IR)
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Veratronitrile
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To synthesize, purify, and isolate veratronitrile from veratraldehyde oxime (IR confirm)
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Aldol condesation
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To synthesize 3-nitrochalcone from m-nitrobenzaldehyde through enolization
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Diazonium salt
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Diazonium salt is synthesized by reacting nitroaniline with sodium nitrite and sulfuric acid
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Adipdic acid IR
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1700(C=O) 3200-3400(OH) 2800-3000(C-H)
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Veratraldehyde oxime IR
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3200-3400(OH) 1550-1650(C=N) ABSENT-1700(C=C)
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Veratronitile IR
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2200(C triple bond N) ABSENT-(OH 3200-3400)
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Aldol condensation melting point
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(144-146°C)
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Diazonium salt chromatography
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Unknown phenol compared to 6 known phenols
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